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The microstructure evolution and optical properties of vacuum combined with hot isostatic pressing(HIP) sintered Tm,Ho:(Lu2/3Sc1/3)2O3 transparent ceramics were studied. The ceramics were sintered in vacuum followed by HIP to obtain Tm,Ho:(Lu2/3Sc1/3)2O3 with high transparency. Changes of microstructure and densification rate due to the vacuum sintering temperature increasing were studied from 1100°C to 1780°C. With the increase of the operating temperature, the densification rate of the ceramics presented nonlinear characteristics. The growth of the grains was remarkably accelerated at higher temperatures (above 1500°C). The in-line transmittance of Tm,Ho:(Lu2/3Sc1/3)2O3 ceramics vacuum sintered at 1780°C followed by HIP at 1700°C exceeded 81.68% at 2090 nm.
Hanlin Yang,Tao Xu,Wei Jing,Bin Kang, andJiachen Liu
"Microstructure evolution during vacuum sintering of Tm,Ho:(Lu2/3Sc1/3)2O3 transparent ceramics", Proc. SPIE 11617, International Conference on Optoelectronic and Microelectronic Technology and Application, 116170L (4 December 2020); https://doi.org/10.1117/12.2584595
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Hanlin Yang, Tao Xu, Wei Jing, Bin Kang, Jiachen Liu, "Microstructure evolution during vacuum sintering of Tm,Ho:(Lu2/3Sc1/3)2O3 transparent ceramics," Proc. SPIE 11617, International Conference on Optoelectronic and Microelectronic Technology and Application, 116170L (4 December 2020); https://doi.org/10.1117/12.2584595