Values of average deformations in local regions of synthesized diamonds are determined using the power Fourier spectrum in the analysis of Kikuchi pattern. The degree of bands blurring on image is related with the deformation, which are quantitatively described through the changes of average radial period of the energy spectrum. The planar distribution of deformations is allowed to determine anisotropy by the magnitude and direction in the crystal.
Аn analysis of the structure formation of concrete composites, compressive strength of which exceeds 120 MPa and a quantitative analysis of their qualitative composition and hydration products by X-ray diffraction, x-ray spectral analysis and electron microscopy. The main factors affecting the physicomechanical parameters of the complex of various nanofillers and the formation of a denser cement stone structure, which mainly includes calcium hydrosilicates, calcium silicate hydroaluminates and hydroaluminates of various basicity, are studied.
The defect structure of p-CdTe:Cl single crystals and MoOx/p-CdTe/MoOx heterostructures based on them were investigated by high-resolution X-ray diffractometry methods. Different models of dislocation systems were applied, according to which the densities of dislocations were estimated from the Wilson-Hall plot. It is shown that the application of the MoOx layer significantly affects the density of dislocations and their influence on the electrical and spectroscopic properties of heterostructures is estimated
Crystal and magnetic domain structures of iron garnet films with different thicknesses are studied by means of atomic and magnetic force scanning microscopies as well as by means of high-resolution Х-ray diffraction. The model of the garnet films as a set of vertical columns with certain lateral sizes is proposed and substantiated. Within this model, X-ray intensity distributions in the vicinity of the reciprocal lattice points are calculated using the Monte Carlo approach to determine densities of two dislocation types with different Burgers vectors.
X-ray moiré images arising from the interaction of deformation fields formed by two perpendicular rows of concentrated loads on the output surface of the LLL interferometer analyzer are calculated. The dynamics of formation of moiré images in case of change of distance between rows is investigated. The prospect of using the fractal dimension of moiré images calculated on the basis of Fourier spectra is shown.
A new approach for determining the distribution of mean-square deformations in the local regions of single crystals and polycrystals based on the analysis of electron backscatter diffraction images is proposed. The degree of bands blurring in Kikuchi pattern is related with the deformation values, which are quantitatively described through the changes of average radial period and the radial distribution area for the energy spectrum of the image. It is shown that the complex use of the power Fourier spectrum method in addition to the two-dimensional Fourier transform method create additional opportunities for determination of the influence of technological parameters on the structural homogeneity and the degree of perfection of studied crystals.
The degree of structural perfection of CdTe:Cl single crystals was estimated by methods of high-resolution Xray diffractometry. Two possible systems of dislocations that consists of two sets of complete 60-degree dislocations and Frank partial dislocations were investigated with the use of Krivoglaz kinematic theory and Monte Carlo method. The density of dislocations that provides correspondence between experimental and simulated reciprocal space maps is determined.
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