This work introduces first time fabricated spun silica microstructured optical fiber (MOF) with inclusion seven GeO2-doped capillaries, placed in the central part of MOF cross-section, and induced twisting. While Part I discussed technological issues for manufacturing of described complicated twisted fiber optic structure, presented some pilot samples of described MOFs with various twisting order and measured their transmission spectra, Part II describes some results of results of experimental researches, performed for successfully manufactured twisted MOF pilot samples with typical hexagonal geometry under hole radius 4.40 μm and pitch 9.80 μm, outer “telecommunication” diameter 125 μm, and center part, formed by seven hollow GeO2-doped ring cores with inner radius 2.50 μm, pitch 8.80 μm and refractive index difference Δn=0.030 with induced twisting 130, 300 and 730 revolutions per meter. Following test series were performed: measurements of far-field laser beam profiles, some attempts of fusion splicing of typical telecommunication optical fibers and fabricated MOF with insertion loss estimation, and spectral response measurements of both single and group WDM (Wavelength Division Multiplexing)-channels of commercially available telecom WDM-system under inclusion of 2 m length MOF into various spans of short-range lab fiber optic link.
This work presents results of test series, performed for earlier on designed and successfully fabricated twisted silica fewmode microstructured optical fibers (MOF) with six GeO2-doped cores. While Part I introduces results of differential mode delay map measurements, Part II is focused on researches of spectral responses, measured for fiber Bragg gratings, recorded in these multi-core MOFs with core graded refractive index profiles and induced twisting 100 revolutions per meter. Specially setup for spectral response measurement for described complicated fiber optic element was developed, that provides selected alignment of matching singlemode optical fiber with particular single core of MOF via free space and reducing of reflection by precision 8 angle cleaving. Comparing analysis of measured spectral responses confirmed written FBGs in 2 of 6 cores, and demonstrated potentiality of fabricated complicated structure, containing multi-core MOF with FBG, for applications in multichannel fiber optic sensors with spatial division multiplexing technique.
This work introduces first time fabricated spun silica microstructured optical fiber (MOF) with inclusion of seven GeO2-doped capillaries, placed in the central part of MOF cross-section, and induced twisting up to 730 revolutions per meter. Part I discusses technological issues for manufacturing of described complicated twisted fiber optic structure, while Part II presents some results of test series, performed for successfully manufactured twisted MOF pilot samples with typical hexagonal geometry under hole radius 4.40 μm and pitch 9.80 μm, outer “telecommunication” diameter 125 μm, and center part, formed by seven hollow GeO2-doped ring cores with inner radius 2.50 μm, pitch 8.80 μm and refractive index difference Δn=0.030. Following measurements were performed: measurements of transmission spectra under various twisting order, far-field laser beam profiles, some attempts of fusion splicing of typical telecommunication optical fibers and fabricated MOF with insertion loss estimation, and spectral response measurements of both single and group WDM (Wavelength Division Multiplexing)-channels of commercially available telecom WDM-system under inclusion of 2 m length MOF into various spans of short-range lab fiber optic link.
This work presents results of test series, performed for earlier on designed and successfully fabricated silica few-mode microstructured optical fibers (MOF) with six GeO2-doped cores, induced twisting 100 revolutions per meter, typical “telecommunication” outer diameter 125 μm, core diameter 8.7 μm, air hole diameter 4.6 μm, pitch 7.2 μm, and core quasi-step / graded refractive index profiles with height 0.0360/0.0275, respectively. Part I introduces attempts for splicing of typical telecommunication optical fibers and fabricated samples of MOFs by commercially available field arc fusion splicer kits and results of differential mode delay map measurements, performed for laser excited large core (multimode) optical fibers with core diameters 50 and 100 μm, jointed via free space to described above 2 m long pilot samples of 6-GeO2-core MOFs at both receiving and transmitting ends under laser-excited gaussian optical pulse launching with precision offset conditions, while Part II is concerned with researches of spectral responses, measured for fiber Bragg gratings, recorded in these MOFs.
This work presents overview of technological issues concerned with drawing of twisted silica microstructured optical fibers. We present results of drawing tower modifications with developed and verified technological modes, that provide fabrication of silica microstructured optical fibers with induced chirality up to extremely high twisting order of 800 revolutions per meter (rpm). Thus, a work package using the original designer technical solutions for upgrade the adapter for supplying overpressure to the cane holes of the microstructured optical fiber (MOF) was carried out. Hence, the target increase in the twisting speed in the cane feed unit to 2000 rpm is ensured while simultaneously target overpressure feeding to the cane holes, which prevents the hole collapsing in the process of MOF drawing. The reliability of the adapter design and the high reproducibility of the specified cross section structure for the MOF at lengths of more than 50 meters with a twist period of 500 rpm have been experimentally confirmed. For the first time in the Russian Federation, prototypes of "stable" chiral MOF lengths (more than 50 m) of a different configuration with a maximum induced twisting of 500 rpm and MOFs prototypes with structure stability at lengths of less than 50 m with a strongly induced chirality of up to 790 rpm were fabricated. The geometric patterns of these fibers are also presented in this work.
We developed and characterized luminescent temperature sensors with a simple construction based on YAG : Ln3 + (Ln = Nd, Yb, Ce) nanocrystals and silica multimode optical fibers. Lanthanide-doped nanocrystals 40 to 60 nm in size were synthesized in the form of powders using the modified Pechini method. The obtained materials exhibited high sensitivity of luminescence intensity to temperature variations at wavelengths of 550 nm (YAG : Ce3 + ), 1030 nm (YAG : Yb3 + ), and 1064 nm (YAG : Nd3 + ) in the temperature range 50°C to 600°C. Additionally, we offered a method to eliminate influence of vibration on accuracy of temperature measurements by adding SiO2 sol to powders after their synthesis in sensitive elements.
The polymer-salt method was applied to synthesize nanoscale Gd2O3:Nd3+ phosphors in the form of thin films on the inner surfaces of capillaries which organize the structure of a silica hollow-core anti-resonant optical fiber. To obtain luminescing centers, the preform of a hollow-core anti-resonant optical fiber was impregnated with a homogeneous mixture of Gd(NO3)3 and NdCl3 dissolved in water and organic solvent (polyvinylpyrrolidone). This procedure was followed by a few post-processing steps, including drying of the impregnated preform in normal conditions and its thermal treatment at temperature 1000 °C. As a result, Gd2O3:Nd3+-based thin films were produced inside the capillaries. Finally, the modified preform was drawn into the hollow-core anti-resonant optical fiber of 120 μm in diameter at temperature 1850 °C. The analysis of crystallographic structure of the initial Gd2O3:Nd3+ nanopowder and the same nanophosphor inside the fabricated fiber revealed the absence of structural and phase transformations of synthesized nanocrystals with an average size 35 nm after drawing. The data on spectral-luminescent properties of the fabricated fiber confirmed the presence of Gd2O3:Nd3+ nanophosphors in silica glass with the main emission peak at wavelength 1064 nm. Presented method of modifying the structure of a hollow-core anti-resonant optical fiber allows formation of active silica layers without using technologically complicated and expensive CVD processes.
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